GIA Pearl Research
Pearls - The Queen of Gems
Prized by many cultures throughout history and frequently referred to as “The Queen of Gems,” pearls have long been one of the most sought-after gemstones in both the jewelry industry and the world at large. Their unique appearance and the affordability of cultured pearls in the market have allowed their popularity to grow exponentially over the years.
Produced by many mollusk species mainly from the Bivalvia and Gastropoda classes, pearls are made of calcium carbonate in the form of aragonite or calcite, through biomineralization process similar to their host shells. In addition, they also contain a small amount of organic matrix and have excellent mechanical properties; they are truly unique and considered as the most important organic gemstone throughout human history. For an overview of various types of pearls found in nature and used for culturing practices, please watch the following GIA Knowledge Sessions Webinar:
Pearl Identification: Natural vs. Cultured
Before the creation of the first commercially successful cultured pearls in the early twentieth century, pearls were so rare and expensive that they were reserved almost exclusively for the very rich, the royal families, and the gods. Not surprisingly, as demand for natural pearls increased, supply gradually diminished. A desire to satisfy the passions for these treasured biogenic gems around the world led to the commercial development of cultured pearls.
GIA had a long history of pearl testing that can be traced back to 1930s, when Japanese akoya cultured pearls were successfully commercialized and it became critical for gemological laboratories to be able to separate natural pearls from their cultured counterparts. Many types of mollusk species can produce natural and cultured pearls so thorough gemological characterization of known samples from various localities and origins around the global is an essential part of GIA’s pearl research. Some examples of such studies are shown in the following links.
- Internal Structures of Known Pinctada maxima Pearls: Cultured Pearls from Operated Marine Mollusks (gia.edu)
- Internal Structures of Known Pinctada maxima Pearls: Natural Pearls from Wild Marine Mollusks (gia.edu)
- Vietnam: Shell Nuclei, Pearl Hatcheries, and Pearl Farming | Gems & Gemology (gia.edu)
- Gemological and Chemical Characteristics of Natural Freshwater Pearls from the Mississippi River System | Gems & Gemology (gia.edu)
- The Gemological Characteristics of Pipi Pearls Reportedly from Pinctada maculata | Gems & Gemology (gia.edu)
- Non-Bead-Cultured Pearls from Pinctada margaritifera | Research & News (gia.edu)
- Bead-Cultured and Non-Bead-Cultured Pearls from Lombok, Indonesia (gia.edu)
- Observations on Pearls Reportedly from the Pinnidae Family (Pen Pearls) | Gems & Gemology (gia.edu)
- Natural Pearls from Australian Pinctada Maxima | Gems & Gemology (gia.edu)
- The Current Status of Chinese Freshwater Cultured Pearls | Gems & Gemology (gia.edu)
Color Treatments and Processes
Detection of treatments, particularly color modification, has been an important part of pearl identification since the early days of GIA. Pearls can be treated into black or golden colors to imitate the Tahitian and golden South Sea cultured pearls in the market, and the treatment techniques have been improved significantly over time, which now requires gem labs to employ more advanced instruments for treatment detection. In addition, pearls may be subjected to routine processes such as bleaching, maeshori (luster enhancement), and optical brightening that can improve their appearances. GIA has developed novel techniques that can identify these post-harvest treatments and processes applied on pearls. Some studies of such applications are listed below.
- Identification of “Chocolate Pearls” Treated by Ballerina Pearl Co. | Gems & Gemology (gia.edu)
- Spectral Reflectance and Fluorescence Characteristics of Natural-Color and Heat-Treated “Golden” South Sea Cultured Pearls | Gems & Gemology (gia.edu)
- Update on the Identification of Dye Treatment in Yellow or "Golden" Cultured Pearls (gia.edu)
- Identification of “Pistachio” Colored Pearls Treated by Ballerina Pearl Co. | Gems & Gemology (gia.edu)
- Optical Whitening and Brightening of Pearls: A Fluorescence Spectroscopy Study | Gems & Gemology (gia.edu)
- Rapid detection of color-treated pearls and separation of pearl types using fluorescence analysis (optica.org)
- Detection of Color Treatment and Optical Brightening in Chinese Freshwater “Edison” Pearls | Gems & Gemology (gia.edu)
Advanced and Unconventional Pearl Testing Techniques
Over the past several decades, pearl testing techniques have developed significantly within gemological laboratories around the world. Currently, a number of advanced instruments are routinely employed for pearl identification at GIA, which include real-time X-ray microradiography, X-ray computed microtomography, UV-Vis spectroscopy, energy-dispersive x-ray fluorescence, laser ablation–inductively coupled plasma–mass spectrometry, Raman spectroscopy, and various photoluminescence and fluorescence spectroscopies. Furthermore, novel and unconventional techniques such as radiocarbon dating and DNA analysis of pearls have also been reported and they can provide useful additional information regarding the origin of pearl samples. Some relevant studies from GIA are listed below.Learn more here about our advanced research instumentation.
- Saltwater Pearls from the Pre- to Early Columbian Era: A Gemological and Radiocarbon Dating Study | Gems & Gemology (gia.edu)
- DNA Techniques Applied to the Identification of Pinctada Fucata Pearls from Uwajima, Ehime Prefecture, Japan | Gems & Gemology (gia.edu)
- DNA Barcoding and Next-Generation Sequencing (NGS) of Freshwater Pearls | Gems & Gemology (gia.edu)
- Provenance Discrimination of Freshwater Pearls by LA-ICP-MS and Linear Discriminant Analysis (LDA) | Gems & Gemology (gia.edu)
- Gemological and Chemical Characteristics of Natural Freshwater Pearls from the Mississippi River System | Gems & Gemology (gia.edu)
- Minerals | Free Full-Text | Raman and Photoluminescence Mapping of Gem Materials (mdpi.com)
Structural Analysis, Biomineralization and Using Pearls as an Environmental Proxy
In addition to the research work in the area of pearl identification, GIA also collaborates and conducts research of this unique biogenic gem material beyond gemology. Some interesting topics we studied in recent years include investigation of nacre nanostructure by analyzing its structural color pattern, using freshwater pearls as a unique proxy for environmental and temperature changes, and discovery of disordered dolomite inside a natural Cassis pearl.
A round Tahitian pearl observed under (a) overhead lighting, and (b) interference enhanced setup.
- Investigation of Nacre Nanostructure by Analyzing Its Structural Color Pattern | Scientific Reports (nature.com)
- Coupling Mineralogy and Oxygen Isotopes to Seasonal Environmental Shifts Recorded in Modern Freshwater Pearl Nacre From Kentucky Lake - Farfan - 2021 - Geochemistry, Geophysics, Geosystems - Wiley Online Library
- Geochemical and mineralogical proxies beyond temperature: Autumn seasons trapped in freshwater nacre - ScienceDirect
- Disordered dolomite as an unusual biomineralization product found in the center of a natural Cassis pearl | PLOS ONE